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Based on the principles of conservation of momentum and energy for X-ray diffraction, a vector description is obtained for the displacement of adjacent subgrain images in reflection topographs. The analysis includes, in addition to those crystal parameters defining the misorientation at a...
Triple orthovanadates MIBaCr2(VO4)3 (where MI = Li, Na or Ag) are synthesised by solid‐state reaction. These compounds are found to have orthorhombically distorted langbeinite structure. The crystallographic parameters of these compounds for an orthorhombic cell with P212121 as the space group...
Laue-case rocking curves of a pair of crystals with nearly equal thickness display a detailed fine structure which is shown to be very suited to the determination of precise values of the atomic scattering factor fg. Preliminary data thus obtained are f440 (AgK) = 5.377 (15) and f440 (Mo K) =...
(±)Rh(en)3(SCN)3 and (+)Rh(en)3(SCN)3, Rh(C2H8N2)3.(SCN)3, C6H24N6Rh.C3N3S3, crystallize in orthorhombic cells. The lattice constants are respectively a = 14.652 (5), b = 14.268 (6), c = 17.480 (6) Å and a = 14.711 (4), b = 13.481 (3), c = 9.166 (2) Å. They are isomorphic with their homologues...
The phases of ammonium nitrate, NH4NO3, doped with small amounts of NiO or CuO have been studied by X-ray and neutron diffraction at various temperatures from 80 to 423 K. NH4NO3 with metal-oxide additives, which are believed to form complexes, exists as a solid solution. Phase IV is stable down...
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