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We report herein the utilization of a vacuum reduction distillation system (VRDS) coupled with mass spectrometry (MS) to characterize chemical transformations in thermal analysis. The system initially designed to monitor metal purification by distillation is applied for the first time to the...
The bend magnet VESPERS beamline on the third generation CLS synchrotron has been equipped with capabilities for X-ray fluorescence (SXRF) excitation with micro-focussed white radiation, as well as with broad and narrow bandpass monochromatised radiation. Using the former two conditions, SXRF...
A novel vapor-generation technique is described for iodine determination in aqueous solutions. The iodide and iodate in the solution are converted to volatile iodine vapor through solution cathode glow discharge induced advanced redox processes. It is achieved by in situ produced highly reactive...
End-on inductively coupled plasma optical emission spectrometry (ICP-OES) of the relative mass distributions in ensembles of spherical SiO 2 particles with small and large size variations is presented. The particles are introduced into the ICP by injection of monodisperse microdroplets generated...
Previous studies have demonstrated both mass-dependent fractionation (MDF) and mass-independent fractionation (MIF) of Hg isotopes in the environment and the potential for their application in biochemistry and geochemistry. However, little has been reported for Hg isotope geochemistry in natural...
A new and highly sensitive method for the determination of 239 Pu in human urine has been developed permitting the reassessment of planchets initially prepared for alpha spectrometry (AS) analysis in the context of internal dosimetry. A set of urine samples (volume: 500 mL) was spiked with known...
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