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Choice of scans in neutron diffraction

Choice of scans in neutron diffraction Neutron-diffraction experiments on single-crystal samples are generally carried out using either an -scan (crystal rotating, detector fixed) or a -2 scan (detector coupled 2:1 to the crystal). In order for the center of the diffracted beam to enter the detector on its centerline at all angular settings of the crystal during the scan of a Bragg reflection, neither of these conventional scanning techniques is optimum. A formula is derived which gives the optimum coupling between the detector and the crystal motions, and it is suggested this mode of scanning should be implemented in performing neutron-diffraction experiments on single crystals. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General Crystallography International Union of Crystallography

Choice of scans in neutron diffraction


Abstract

Neutron-diffraction experiments on single-crystal samples are generally carried out using either an -scan (crystal rotating, detector fixed) or a -2 scan (detector coupled 2:1 to the crystal). In order for the center of the diffracted beam to enter the detector on its centerline at all angular settings of the crystal during the scan of a Bragg reflection, neither of these conventional scanning techniques is optimum. A formula is derived which gives the optimum coupling between the detector and the crystal motions, and it is suggested this mode of scanning should be implemented in performing neutron-diffraction experiments on single crystals.

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Publisher
International Union of Crystallography
Copyright
Copyright (c) 1971 International Union of Crystallography
ISSN
0567-7394
DOI
10.1107/S0567739471001414
Publisher site
See Article on Publisher Site

Abstract

Neutron-diffraction experiments on single-crystal samples are generally carried out using either an -scan (crystal rotating, detector fixed) or a -2 scan (detector coupled 2:1 to the crystal). In order for the center of the diffracted beam to enter the detector on its centerline at all angular settings of the crystal during the scan of a Bragg reflection, neither of these conventional scanning techniques is optimum. A formula is derived which gives the optimum coupling between the detector and the crystal motions, and it is suggested this mode of scanning should be implemented in performing neutron-diffraction experiments on single crystals.

Journal

Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General CrystallographyInternational Union of Crystallography

Published: Nov 1, 1971

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