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Evidence for the Fankuchen effect in neutron diffraction by curved crystals

Evidence for the Fankuchen effect in neutron diffraction by curved crystals Experimental evidence of the Fankuchen effect for neutron diffraction by curved crystals is presented and discussed. The Fankuchen effect consists of a space condensation of neutrons (or X-rays) diffracted by an asymmetrically cut crystal. Theoretical considerations are presented on the Fankuchen effect in the case of ideal mosaic crystals, perfect crystals and ideal curved crystals. This analysis shows that mosaic crystals behave quite differently from perfect crystals. Whereas for perfect crystals the asymmetric cut is expected to induce a real gain in neutron current density, for mosaic crystals no gain is expected. Curved crystals are expected to behave in a similar way to perfect crystals. The experiments were carried out on chemically curved Si crystals. The neutron-diffraction characteristics of a symmetrically cut Si crystal and an asymmetrically cut Si crystal were compared. A gain in the neutron current density of a factor of 4 was observed in the case of the asymmetric crystal. This value is in good agreement with the estimated theoretical value of 4.2. This fact could lead to interesting applications in the selection of monochromatic beams to be used in neutron diffractometry of small biological crystals. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General Crystallography International Union of Crystallography

Evidence for the Fankuchen effect in neutron diffraction by curved crystals

Evidence for the Fankuchen effect in neutron diffraction by curved crystals


Abstract

Experimental evidence of the Fankuchen effect for neutron diffraction by curved crystals is presented and discussed. The Fankuchen effect consists of a space condensation of neutrons (or X-rays) diffracted by an asymmetrically cut crystal. Theoretical considerations are presented on the Fankuchen effect in the case of ideal mosaic crystals, perfect crystals and ideal curved crystals. This analysis shows that mosaic crystals behave quite differently from perfect crystals. Whereas for perfect crystals the asymmetric cut is expected to induce a real gain in neutron current density, for mosaic crystals no gain is expected. Curved crystals are expected to behave in a similar way to perfect crystals. The experiments were carried out on chemically curved Si crystals. The neutron-diffraction characteristics of a symmetrically cut Si crystal and an asymmetrically cut Si crystal were compared. A gain in the neutron current density of a factor of 4 was observed in the case of the asymmetric crystal. This value is in good agreement with the estimated theoretical value of 4.2. This fact could lead to interesting applications in the selection of monochromatic beams to be used in neutron diffractometry of small biological crystals.

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References (1)

Publisher
International Union of Crystallography
Copyright
Copyright (c) 1977 International Union of Crystallography
ISSN
0567-7394
DOI
10.1107/S0567739477000989
Publisher site
See Article on Publisher Site

Abstract

Experimental evidence of the Fankuchen effect for neutron diffraction by curved crystals is presented and discussed. The Fankuchen effect consists of a space condensation of neutrons (or X-rays) diffracted by an asymmetrically cut crystal. Theoretical considerations are presented on the Fankuchen effect in the case of ideal mosaic crystals, perfect crystals and ideal curved crystals. This analysis shows that mosaic crystals behave quite differently from perfect crystals. Whereas for perfect crystals the asymmetric cut is expected to induce a real gain in neutron current density, for mosaic crystals no gain is expected. Curved crystals are expected to behave in a similar way to perfect crystals. The experiments were carried out on chemically curved Si crystals. The neutron-diffraction characteristics of a symmetrically cut Si crystal and an asymmetrically cut Si crystal were compared. A gain in the neutron current density of a factor of 4 was observed in the case of the asymmetric crystal. This value is in good agreement with the estimated theoretical value of 4.2. This fact could lead to interesting applications in the selection of monochromatic beams to be used in neutron diffractometry of small biological crystals.

Journal

Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General CrystallographyInternational Union of Crystallography

Published: May 1, 1977

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