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Mesure de la temperature de Debye de CsI par diffraction de rayons X

Mesure de la temperature de Debye de CsI par diffraction de rayons X The Debye temperature of powdered CsI has been measured at room temperature from continuous diffractometric recording of -filtered Cu K reflexions, using a dead-time correction formula Kouchkovsky, R. de (1974). Acta Cryst. A 30, 406-408 and taking into account the variation with Bragg angle of the K2/K1 intensity ratio. The value determined, 112 plus or minus 3DegreesK at 23 DegreesC, is slightly below the one that can be deduced from elastic moduli (115DegreesK), and in good agreement with the general theoretical predictions. Unfortunately, there is some discrepancy with the value calculated from a frequency distribution curve recently published. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General Crystallography International Union of Crystallography

Mesure de la temperature de Debye de CsI par diffraction de rayons X

Mesure de la temperature de Debye de CsI par diffraction de rayons X


Abstract

The Debye temperature of powdered CsI has been measured at room temperature from continuous diffractometric recording of -filtered Cu K reflexions, using a dead-time correction formula Kouchkovsky, R. de (1974). Acta Cryst. A 30, 406-408 and taking into account the variation with Bragg angle of the K2/K1 intensity ratio. The value determined, 112 plus or minus 3DegreesK at 23 DegreesC, is slightly below the one that can be deduced from elastic moduli (115DegreesK), and in good agreement with the general theoretical predictions. Unfortunately, there is some discrepancy with the value calculated from a frequency distribution curve recently published.

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References (6)

Publisher
International Union of Crystallography
Copyright
Copyright (c) 1974 International Union of Crystallography
ISSN
0567-7394
DOI
10.1107/S0567739474000908
Publisher site
See Article on Publisher Site

Abstract

The Debye temperature of powdered CsI has been measured at room temperature from continuous diffractometric recording of -filtered Cu K reflexions, using a dead-time correction formula Kouchkovsky, R. de (1974). Acta Cryst. A 30, 406-408 and taking into account the variation with Bragg angle of the K2/K1 intensity ratio. The value determined, 112 plus or minus 3DegreesK at 23 DegreesC, is slightly below the one that can be deduced from elastic moduli (115DegreesK), and in good agreement with the general theoretical predictions. Unfortunately, there is some discrepancy with the value calculated from a frequency distribution curve recently published.

Journal

Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General CrystallographyInternational Union of Crystallography

Published: May 1, 1974

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